Article Article
Nondestructive Evaluation of Electroplating-Induced Hydrogen Embrittlement in Cadmium-Coated High-Strength Steel Using Ultrasonic Surface Waves

Development of a nondestructive evaluation (NDE) method to detect nascent hydrogen embrittlement (HE) in electroplated high-strength steel parts is becoming important for the aerospace industry. This research investigates the feasibility of surface acoustic waves (SAWs) measurements to distinguish between cadmium (Cd) plated SAE 4340 steel samples with low and high HE susceptibilities. SAWs were generated with a 10 MHz piezoelectric transducer and detected by line scans via a laser Doppler vibrometer setup. Using signal processing algorithms in MATLAB, SAW velocities as well as attenuation coefficients were estimated. Depth profiles of steel hardness near coatings were also evaluated using Vickers microindentation tests. Average steel hardness in not-baked samples was slightly increased. Cd coatings were characterized by laser and optical microscopy methods. Small variations found in thickness and surface roughness of the Cd coatings among the samples did not significantly affect the NDE results. On average, samples in the not-baked condition (high HE risk) exhibited lower SAW attenuation coefficients compared to immediately baked and late-baked conditions (low HE risk). However, it was not possible to distinguish between the manufacturing conditions of individual samples due to overlaps in attenuation measurement results. SAW velocities as estimated by the cross-correlation method were found to be not sensitive to manufacturing conditions.

DOI: https://doi.org/10.32548/2021.me-04231

References

Abrámoff, M.D., P.J. Magalhães, and S.J. Ram, 2004, “Image Processing with ImageJ,” Biophotonics International, Vol. 11, No. 7, pp. 36–42

ASTM, 2017, ASTM E384: Standard Test Method for Microindentation Hardness of Materials, ASTM International, West Conshohocken, PA, https://doi.org/10.1520/E0384-17

Barrera, O., D. Bombac, Y. Chen, T.D. Daff, E. Galindo-Nava, P. Gong, D. Haley, R. Horton, I. Katzarov, J.R. Kermode, C. Liverani, M. Stopher, and F. Sweeney, 2018, “Understanding and Mitigating Hydrogen Embrittlement of Steels: A Review of Experimental, Modelling and Design Progress from Atomistic to Continuum,” Journal of Materials Science, Vol. 53, pp. 6251–6290, https://doi.org/10.1007/s10853-017-1978-5

Cheeke, J.D.N., 2012, Fundamentals and Applications of Ultrasonic Waves, 2nd edition, Chapter 8, CRC Press

Connolly, G.D., J. Li, and S.I. Rokhlin, 2013, “Fatigue Crack Monitoring in Engine-Grade Titanium Alloy by Dynamic Subtraction of Surface Acoustic Wave Modulation,” NDT & E International, Vol. 55, pp. 47–56, https://doi.org/10.1016/j.ndteint.2013.01.009

de Billy, M., G. Quentin, and E. Baron, 1987, “Attenuation Measurements of an Ultrasonic Rayleigh Wave Propagating Along Rough Surfaces,” Journal of Applied Physics, Vol. 61, No. 6, pp. 2140–2145, https://doi.org/10.1063/1.337972

Doerr, C., J.-Y. Kim, P. Singh, J.J. Wall, and L.J. Jacobs, 2017, “Evaluation of Sensitization in Stainless Steel 304 and 304L Using Nonlinear Rayleigh Waves,” NDT & E International, Vol. 88, pp. 17–23, https://doi.org/10.1016/j.ndteint.2017.02.007

Figueroa, D., and M.J. Robinson, 2008, “The Effects of Sacrificial Coatings on Hydrogen Embrittlement and Re-embrittlement of Ultra High Strength Steels,” Corrosion Science, Vol. 50, No. 4, pp. 1066–1079, https://doi.org/10.1016/j.corsci.2007.11.023

Lakestani, F., J.-F. Coste, and R. Denis, 1995, “Application of Ultrasonic Rayleigh Waves to Thickness Measurement of Metallic Coatings,” NDT & E International, Vol. 28, No. 3, pp. 171–178, https://doi.org/10.1016/0963-8695(95)00010-U

Hasegawa, Y., 1998, “Failures from Hydrogen Attack and their Methods of Detection,” Welding International, Vol. 2, No. 6, pp. 514–521, https://doi.org/10.1080/09507118809447511

Hillier, E.M.K., and M.J. Robinson, 2004, “Hydrogen Embrittlement of High Strength Steel Electroplated with Zinc-Cobalt Alloys,” Corrosion Science, Vol. 46, No. 3, pp. 715–727, https://doi.org/10.1016/S0010-938X(03)00180-X

Johnson, H.H., J.G. Morlet, and A.R. Troiano, 1958, “Hydrogen, Crack Initiation, and Delayed Failure in Steel,” Transactions of the Metallurgical Society of AIME, Vol. 212, pp. 528–536

Krüger, S.E., J.M.A. Rebello, and P.C. de Camargo, 1999, “Hydrogen Damage Detection by Ultrasonic Spectral Analysis,” NDT & E International, Vol. 32, No. 5, pp. 275–281, https://doi.org/10.1016/S0963-8695(98)00052-8

Laliberté-Riverin, S., J. Bellemare, F. Sirois, and M. Brochu, 2020, “Internal Hydrogen Embrittlement of Pre-cracked, Cadmium-Plated AISI 4340 High Strength Steel with Sustained Load Tests and Incremental Step-Loading Tests,” Engineering Fracture Mechanics, Vol. 223, https://doi.org/10.1016/j.engfracmech.2019.106773

Nagumo, M., 2004, “Hydrogen Related Failure of Steels – a New Aspect,” Materials Science and Technology, Vol. 20, No. 8, pp. 940–950, https://doi.org/10.1179/026708304225019687

Oriani, R.A., and P.H. Josephic, 1974, “Equilibrium Aspects of Hydrogen-Induced Cracking of Steels,” Acta Metallurgica, Vol. 22, No. 9, pp. 1065–1074, https://doi.org/10.1016/0001-6160(74)90061-3

Oriani, R.A., and P.H. Josephic, 1980, “Effects of Hydrogen on the Plastic Properties of Medium-Carbon Steels,” Metallurgical Transactions A, Vol. 11, pp. 1809–1820, https://doi.org/10.1007/BF02655096

Ruiz, A., and P.B. Nagy, 2004, “Laser-Ultrasonic Surface Wave Dispersion Measurements on Surface-Treated Metals,” Ultrasonics, Vol. 42, Nos. 1–9, pp. 665–669, https://doi.org/10.1016/j.ultras.2004.01.045

SAE, 2016, AMS6415U: Aerospace Material Specification, Steel, Bars, Forgings, and Tubing 0.80Cr - 1.8Ni - 0.25Mo (0.38 - 0.43C) (SAE 4340), SAE International, https://doi.org/10.4271/AMS6415U

Sriraman, K.R., S. Brahimi, J.A. Szpunar, and S. Yue, 2013, “Hydrogen Embrittlement of Zn-, Zn–Ni-, and Cd-coated High Strength Steel,” Journal of Applied Electrochemistry, Vol. 43, pp. 441–451, https://doi.org/10.1007/s10800-013-0529-2

Takai, K., and R. Watanuki, 2003, “Hydrogen in Trapping States Innocuous to Environmental Degradation of High-Strength Steels,” ISIJ International, Vol. 43, No. 4, pp. 520–526, https://doi.org/10.2355/isijinternational.43.520

Wang, P.-N., and S.-H. Chang, 2018, “Effect of the Mechanical Properties and Corrosion Behaviors of Nickel-Cadmium Duplex Electroplated AISI 4340 Steel by Using Various Solid Solution Treatments,” Materials Transactions, Vol. 59, No. 3, pp. 406–411, https://doi.org/10.2320/matertrans.M2017282

Warren, P.D., C. Pecorari, O.V. Kolosov, S.G. Roberts, and G.A.D. Briggs, 1996, “Characterization of Surface Damage via Surface Acoustic Waves,” Nanotechnology, Vol. 7, No. 3, pp. 295–301, https://doi.org/10.1088/0957-4484/7/3/020

Ye, C., W. Kan, Y. Li, and H. Pan, 2013, “Experimental Study of Hydrogen Embrittlement on AISI 304 Stainless Steels and Rayleigh Wave Characterization,” Engineering Failure Analysis, Vol. 34, pp. 228–234, https://doi.org/10.1016/j.engfailanal.2013.07.021

Zamanzadeh, M., A. Allam, C. Kato, B. Ateya, and H.W. Pickering, 1982, “Hydrogen Absorption during Electrodeposition and Hydrogen Charging of Sn and Cd Coatings on Iron,” Journal of The Electrochemical Society, Vol. 129, No. 2, pp. 284–289, https://doi.org/10.1149/1.2123813

Zeitvogel, D.T., K.H. Matlack, J.-Y. Kim, L.J. Jacobs, P.M. Singh, and J. Qu, 2014, “Characterization of Stress Corrosion Cracking in Carbon Steel Using Nonlinear Rayleigh Surface Waves,” NDT & E International, Vol. 62, pp. 144–152, https://doi.org/10.1016/j.ndteint.2013.12.005

Zielinski, A., and N.F. Fiore, 1982, “Surface Ultrasonic Studies of Time-Dependent Dislocation Pinning by H Atoms in F.C.C. Stainless Alloys,” Acta Metallurgica, Vol. 30, No. 3, pp. 743–748, https://doi.org /10.1016/0001-6160(82)90124-9

 

Metrics
Usage Shares
Total Views
234 Page Views
Total Shares
0 Tweets
234
0 PDF Downloads
0
0 Facebook Shares
Total Usage
234